The synthetic chemistry laboratory is equipped with chemical fume hoods, balances, heating mantles, stirrers, refrigerators, freezers, Buchi R-300 rotary evaporators with V-300 vacuum pumps, a lab oven, a Melting Point Apparatus, a Biotage Microwave Synthesizer, a ACCQPrep HP150 Prep HPLC System, and a CombiFlash NextGen 300+ Automated Flash Chromatography System.
Biotage®Initator+ Microwave System
Manufacturer: Biotage®
Description/Applications: Biotage® Initator+ Microwave Systemwith Robot Eight Automation for Microwave Assisted Organic Synthesis
Supporting Documents: Instruction Manual
CombiFlash NextGen 300+
Manufacturer: Teledyne ISCO
Description/Applications: The CombiFlash NextGen 300+ comes standard with all options installed. Flow rate range is from 1 to 300 mL/min at operating pressures up to 300 psi (20 bar). The system is fitted with a solid load injection valve that can be bypassed if you decide to perform a liquid injection.
Supporting Documents: Instruction Manual
ACCQPrep HP150 Prep HPLC System
Manufacturer: Teledyne ISCO
Description/Applications: ACCQPrep HP150 Prep HPLC System with 200-400nm UV variable wavelength detector. 1-150 ml/min. Up to 6000 psi (400 bar).
Supporting Documents: Instruction Manual
BUCHI Rotavapor™ R-300
Manufacturer: BUCHI
Description/Applications: BUCHI Rotavapor™ R-300 Rotary Evaporator with Controller and V-300 Pump
Supporting Documents: Instruction Manual
In addition to these core facilities, the core has access to the school Shared Analytical Facility, which includes NMRs a Varian Inova 400, Thermo Fisher Q-Exactive (LC-MS/MS), and other essential analytical instruments such as Sciex 6500+ (Triple quad/ion trap, LC-MS/MS), Bruker Rapiflex (MALDI-TOF-TOF)
Oxford NMR AS400
Manufacturer: Oxford
Location: PSC 402G
Description/Applications: Two-channel superconducting 400 MHz NMR Spectrometer that produces very high-resolution data. Liquid and solid samples are achievable for structural analysis and identification of organic molecules.
Supporting Documents: SOP Document